D2-phaser-中文手册

06/07/2020BrukerConfidential1D2Phaser基本中文操作手冊06/07/2020BrukerConfidential2外觀系統指示燈X-ray指示燈LCD螢幕門把&門鎖鍵盤&滑鼠06/07/2020BrukerConfidential3開機確定鑰匙轉向右邊06/07/2020BrukerConfidential4開機接上100~240VAC的電源,按下黑色鈕至”I”06/07/2020BrukerConfidential5開機直到出現windows登入畫面,輸入密碼”password”,然後按”Enter”點選DIFFRAC.Measurement,出現login視窗後,不用輸入password,直接按”O.K”06/07/2020BrukerConfidential6開機一開機系統會自動把TwoTheat做歸位,除了PHI以外,這時就可把Request打勾,然後按”Init”做歸位,如果沒問題都是綠色打勾符號,系統待命量測只要一開始做歸位即可,其他關機或量測完都不需要06/07/2020BrukerConfidential7關機X-ray按下”Off”,X-ray指示燈熄滅Off06/07/2020BrukerConfidential8關機把DIFFRACMeasurement程式關閉,然後將windows正常關閉(跟一般電腦一樣程序)等待畫面出現”Itisnowsafetoturnoffyourcomputer”按下後方黑色鈕至”0”06/07/2020BrukerConfidential9放置樣品打開外蓋,把黑色鈕往上頂06/07/2020BrukerConfidential10放置樣品確定Slit是否正確及Airscatterscreen方向是否O.K06/07/2020BrukerConfidential11放置樣品(配置ScintilationCounter)另外一邊Slit是否正確,Nifilter確定放置如何搭配:DS:1mmor0.6mm,AS:1mmor0.6mm,Nifilter,RS:0.2mmor0.1mmDSASNiRS06/07/2020BrukerConfidential12放置樣品(配置Lynxeye偵測器)確定有放置Soller&Nifilter06/07/2020BrukerConfidential13放置樣品AirScatterScreen有分1mm&3mm06/07/2020BrukerConfidential14放置樣品放置樣品,將黑色圓心往下拉,再來將樣品座置入,往上推回即可06/07/2020BrukerConfidential15快速量測(需手動儲存掃描完的圖形)範例:步驟一至Commander,按X-ray“ON”,X-ray指示燈亮起06/07/2020BrukerConfidential16快速量測(需手動儲存掃描完的圖形)如果樣品要旋轉,輸入轉速(15,30,60rpm),然後按”Set”06/07/2020BrukerConfidential17快速量測(需手動儲存掃描完的圖形)此目的在於先初掃一次,確定peak集中在那一區域範例:步驟一Scantype:CoupledTheta/TwoThetascan(符合布拉格定律)範圍:34.7~35.7度,間距:0.005度,間距掃描時間:0.5s確定都O.K,之後再按”Start”06/07/2020BrukerConfidential18快速量測(需手動儲存掃描完的圖形)結果出來之後,按”FileSaveLastMeasuredRawfile存檔類型請存成”V3Rawfileandbrmlfile”,不然無法轉成文字檔06/07/2020BrukerConfidential19XRDWizard(編輯掃描參數)點選XRDWizard,出現login視窗後,不用輸入password,直接按”O.K”06/07/2020BrukerConfidential201.更新時間2.輸入使用者3.樣品名稱4.確認後,按”OK”此頁設定為參考用,並不影響樣品量測06/07/2020BrukerConfidential21此頁為系統規格,直接按”OK”06/07/2020BrukerConfidential22此頁為Slit設定,為參考用,不影響量測,直接按”OK”06/07/2020BrukerConfidential23選擇偵測器,請確定選擇是”Lynxeye1Dmode”,再選擇”entervalue”,在右邊空格輸入”5”確定後,按”OK”06/07/2020BrukerConfidential241.掃描方式選擇2.掃描模式選擇,建議為”Continuousscan3.樣品旋轉選擇4.確認後,按”OK”06/07/2020BrukerConfidential251.設定量測參數範圍:Start,Stop,StepSize,Time/Step2.確認後,按”OK”06/07/2020BrukerConfidential261.電壓,電流設定2.確認後,按”OK”06/07/2020BrukerConfidential27設定完後,到File-SaveAs,把參數存檔,副檔名為”bsml”,存完之後,程式就可以結束.06/07/2020BrukerConfidential28執行掃描參數回至MeasurementCenter,到StartJOBS”頁面選擇編輯好的掃描參數,再輸入掃描完的檔案名稱,再按右下方的”StartJob”掃完之後,程式會自動存成”Rawfileandbrmlfile”06/07/2020BrukerConfidential29中斷掃描程序如果臨時要中斷,選擇要中斷的程式,然後按紅色”Stop”06/07/2020BrukerConfidential30簡易保養(冷卻水)確定後方冷卻水是否在正常準位,如果接近min位準,就需要加冷卻水準備Bruker的冷卻罐裝水06/07/2020BrukerConfidential31簡易保養(冷卻水)鬆掉螺絲,打開蓋子,抽出冷卻罐06/07/2020BrukerConfidential32簡易保養(冷卻水)加入冷卻水,蓋上後蓋06/07/2020BrukerConfidential33簡易保養(清潔空氣濾心)