第七章TOC-V实验步骤

TOC-V21.2.3.4.5.SSM-5000A318KHPTC8IC8ICTOC4TC1000ppmTC1)KHP105—12012)2.125g3)1L4)5)425IC1000ppmIC1)NaHCO32Na2CO3280—29012)3.50g4.41g3)1L4)5)426TN1000ppmTN1)KNO3105-11032)7.219g3)1L4)5)427TCTN100ppmTC100ppmTN1)1000ppmTC1000ppmTN100ml1L2)25ml2MHCl0.05M3)4)4282MHCl1)HCl37%12M50mL250mL62)250ml3)925%w/wH3PO41)H3PO485%1.6952)50ml250ml3)250ml4)10160g15mL2500mL2411100mL85%500mL12131415TOCTOC1612DOC3ASI-5000AASI-V174)5)6)18500ppm5%0.1%19TCICICTCIC200.5ppm500ppb:NPOCTC-IC/52-31MHCl/100ml21TCICPt0.5%TOC500ppbPt0.5%TOC500ppbIC25%w/wH3PO450ml85%H3PO4250ml22TOC-V24ml9340ml68TOC125ml24ASI-V23:NPOCICPOC10mg/lpH724ParafilmASI-5000ATOC-V2525mmASI-5000A25HCl2MpH2—3pH10ppbNPOCCO2NPOC26TOC-VNPOCASI-VTC273(1)(2)5mm(3)TOC100mmTOC28TOC(1)(2)(3)(4)130mm29TOC/TN(1)(2)5mm(3)TOC140mm(4)(5)10mm30(1)(2)1mm31(3)(4)32(1)(2)(3)(4)(5)(6)33(1)(2)“Hi”34IC12[[34200mL/min5635412150ml/min34TOC-ControlV5NewSystem6TOC-ControlVSampleTableEditor7Connect30368NewCalibrationCurveNewMethodInsertSampleNewControlSampleTemplate9NewSampleRun3710InsertCalibrationCurveSampleControl12Start13ViewSampleWindow1415InstrumentStandby1138TOCTCICTNNPOCTC0400ppbTCICTOC=TC-ICTNTOC=TC-ICNPOCTCICTOCTOC=TC-ICNPOCTCIC720680680TC/TNTN:0.1−−4000ppm20ppb25,000ppm150ppb25,000ppmTC/TN395SSM-5000ASSM-5000A500mL/minSSM-5000ATOC-VTOC-VCPH150mL/minTOC-VWP200mL/minSSM-5000A40TCTC90020900206002041ICIC2-3M1042IC85%14.60mol/L124.87mol/LIC43C6H12O6TCC8H9NOAcetoanilideN-phenylacetamideCASNumber103-84-444Na2CO3CaCO3IC4530mgCTC75mg82.5mg20mgCIC176.7mg46SSM-5000ATC/IC2BackgroundMonitor]247IC48TC0.130mg1-20gIC0.120mgC1g0.5g