与农药剂型相关的控制指标

与农药剂型相关的控制项目原药technicalmaterial(TC)母药technicalconcentrate(TK)Declaredcontenting/kgorg/lat20±2°CToleranceupto25±15%ofthedeclaredcontentfor“homogeneous”formulations(EC,SC,SL,etc.),or±25%for“heterogeneous”formulations(GR,WG,etc.)above25upto100±10%ofthedeclaredcontentabove100upto250±6%ofthedeclaredcontentabove250upto500±5%ofthedeclaredcontentabove500upto900±25g/kgorg/labove900upto1000theminimumcontent,only,isdeclared.NoteIneachrangetheupperlimitisincluded1.粉剂（DP）DUSTABLEPOWDERS1)水分含量Water(MT30.5)Maximum:......g/kg.2）细度（通过75μm试验筛）Drysievetest(MT59.1)Maximum:5%retainedona75μmtestsieve.3）酸碱度（以H2SO4或NaOH计）或pH范围Acidityand/orAlkalinity(MT191)orpHrange(MT75.3)Maximumacidity:......g/kgcalculatedasH2SO4.Maximumalkalinity:......g/kgcalculatedasNaOH.pHrange:......to......4）其他Stabilityatelevatedtemperature(MT46.3)2.乳油(EC)Emulsifiableconcentrates1）水分含量Water(MT30.5)Maximum:......g/kg.2）酸碱度（以H2SO4或NaOH计）或pH范围Acidityand/orAlkalinity(MT191)orpHrange(MT75.3)Maximumacidity:......g/kgcalculatedasH2SO4.Maximumalkalinity:......g/kgcalculatedasNaOH.pHrange:......to......3）乳液稳定性Emulsionstabilityandre-emulsification(MT36.1.1,MT36.3orMT183)TimeafterdilutionLimitsofstability,MT36.1,MT36.30hInitialemulsificationcomplete0.5hCream,maximum:......ml2.0hCream,maximum:......mlFreeoil,maximum:......ml24hRe-emulsificationcomplete24.5hCream,maximum:......mlFreeoil,maximum:......mlNote:inapplyingMT36.1or36.3,testsafter24harerequiredonlywhereresultsat2hareindoubtTimeafterdilutionLimitsofstability,MT1832minACreadingmaximum......7to32minACreadingsimilartoabove(nomajorincrease,declineorfluctuation)Note:inapplyingMT183,initialACreadingwillbe1inmostcases4）其他Persistentfoam(MT47.2)(Note7)Maximum:......mlafter1min.StoragestabilityStabilityat0°C(MT39.3)Afterstorageat0±2°Cfor7days,thevolumeofsolidand/orliquidwhichseparatesshallnotbemorethan0.3ml.Stabilityatelevatedtemperature(MT46.3)Afterstorageat54±2°Cfor14days,thedeterminedaverageactiveingredientcontentmustnotbelowerthan......%relativetothedeterminedaveragecontentfoundbeforestorageandtheformulationshallcontinuetocomplywiththeclausesfor:-acidity,alkalinity,pHrange,-emulsionstabilityandre-emulsification3.可湿性粉剂(WP)WETTABLEPOWDERS1）水分含量Water(MT30.5)Maximum:......g/kg.2）酸碱度(以H2SO4或NaOH计)或pH范围Acidityand/orAlkalinity(MT191)orpHrange(MT75.3)Maximumacidity:......g/kgcalculatedasH2SO4.Maximumalkalinity:......g/kgcalculatedasNaOH.pHrange:......to......3）悬浮率Suspensibility(MT15.1,MT177,MT184)(Notes5&6)Aminimumof......%ofthe......[ISOcommonname]contentshallbeinsuspensionafter30mininCIPACStandardWaterDat30±2°C.4）湿润时间Wettability(MT53.3)Theformulationshallbecompletelywettedin......minwithoutswirling.5）细度（通过45μm试验筛）Wetsievetest(MT185)Maximum:......%retainedona45μmtestsieve.6）其他Stabilityatelevatedtemperature(MT46.3)Afterstorageat54±2°Cfor14days,thedeterminedaverageactiveingredientcontentmustnotbelowerthan......%relativetothedeterminedaveragecontentfoundbeforestorageandtheformulationshallcontinuetocomplywiththeclausesfor:-acidity/alkalinity/pHrange,-wetsievetest,-suspensibility,-wettability,Persistentfoam(MT47.2)Maximum:......mlafter1min.4.颗粒剂(GR)Granules1）水分含量2）松密度和堆密度（视需要）3）酸碱度(以H2SO4或NaOH计)或pH范围4）粒度范围5）脱落率或强度6）其他5.悬浮剂（SC）Aqueoussuspensionconcentrates1）酸碱度（以H2SO4或NaOH计）或pH范围Acidityand/orAlkalinity(MT191)orpHrange(MT75.3)Maximumacidity:......g/kgcalculatedasH2SO4.Maximumalkalinity:......g/kgcalculatedasNaOH.pHrange:......to......2）湿筛试验（通过75μm试验筛）Wetsievetest(MT185)Maximum:......%oftheformulationshallberetainedona......μmtestsieve.3）悬浮率Suspensibility(MT184)Aminimumof......%ofthe......[ISOcommonname]contentshallbeinsuspensionafter30mininCIPACStandardWaterDat30±2°C.4）倾倒性Pourability(MT148.1)Maximumresidue:......%.5）持久起泡性Persistentfoam(MT47.2)(Note9)Maximum:......mlafter1min.*Spontaneityofdispersion(MT160)Aminimumof......%ofthe......[ISOcommonname]contentshallbeinsuspensionafter5mininCIPACStandardWaterDat30±2°C*Particlesizedistribution(MT187)…%ofparticlesshallbeintherange…to…*Viscosity(MT192)Theviscosityshallbeintherange…to….6）其他StoragestabilityStabilityat0°C(MT39.3)Afterstorageat0±2°Cfor7days,theformulationshallcontinuetocomplywithclausesfor:-suspensibility,-wetsievetest,Stabilityatelevatedtemperature(MT46.3)Afterstorageat54±2°Cfor14days(Note11),thedeterminedaverageactiveingredientcontentmustnotbelowerthan......%relativetothedeterminedaveragecontentfoundbeforestorageandtheformulationshallcontinuetocomplywiththeclausesfor:-acidity/alkalinity/pHrange,-pourability,-spontaneityofdispersion,-suspensibility,-wetsievetest,6.水剂(AS)aqueoussolution1）水不溶物含量2）酸碱度(以H2SO4或NaOH计)或pH范围3）稀释稳定性4）其他7.可溶粉剂(SP)Watersolublepowders1）水分含量Water(MT30.5)Maximum:......g/kg.2）酸碱度(以H2SO4或NaOH计)或pH范围Acidityand/orAlkalinity(MT191)orpHrange(MT75.3)Maximumacidity:......g/kgcalculatedasH2SO4.Maximumalkalinity:......g/kgcalculatedasNaOH.pHrange:......to......3）溶解程度和溶液稳定性（通过75μm试验筛）Degreeofdissolutionandsolutionstability(MT179)Residueofformulationretainedona75μmtestsieveafterdissolutioninCIPACStandardWaterDat30±2°C:Maximum:......%after5min.Maximum:......%after18hou