安捷伦液相培训-新版软件使用(Chemstation-IR)

AgilentOpenLABCDSChemStation介绍2AgandaOpenLABCDS产品架构简介3Page3AgilentOpenLABCDS单机版Page3OpenLABCDS单机版OpenLABCDS单机版Instrument3rdpartyDriverLCDriverInstrument4Page4AgilentOpenLAB完整版系统架构AICAICClientClientClientClientOpenLAB共享服务ECM/ELN服务器ServercoreAICInstrument3rdpartyDriverInstrument3rdpartyDriverAICGCDriverInstrumentLCDriverInstrument5IntelligentorLegacyReportingIntelligentReportingisonlyavailablewithOpenLab.YoumustselectthisoptionwhenconfiguringtheinstrumentinOpenLab.126AgandaOpenLABCDS设计架构设计介绍7DirectoryStructureofChemStationSoftwareInstrumentfolders:datafiles,methods,sequencefiles,etc.ExecutionfilesandmacrosReportTemplatesSpectralLibraries8TermsandDefinitions•StoredinChem32\1\Methodswhere1indicatesinstrumentnumber.•Remainsunchangedduringacquisitionanddataanalysis.MasterMethod•StoredinChem32\1\Sequence.•Usedtorunasequence,butnotusedforreprocessing.SequenceTemplate•Containerorfolderofdatafiles,sequencemethod,reporttemplates,logfiles,etc..•Maybecreatedautomaticallybyrunningasequenceorthroughself-assembly.•SequencereprocessingisdoneusingtheResultSet.ResultSet•MasterMethodcopiedintotheresultset.•Usedforreprocessing.SequenceMethod•StoredinChem32\Repstyle.•CopyofIntelligentReporttemplatesstoredinResultSet.ReportTemplate9ChemStationFoldersMasterMethodsSequenceTemplatesIndividualDataFilesandResultSetsTemporaryFiles10DataOrganizationConcept–ResultSetAtthestartofanalysisanewuniquefolderiscreatedwithprivatecopyofthemastermethodandsequencetemplate.Astheanalysisproceeds,allfilesassociatedwiththeanalysisorsequenceofanalysesarestoredinthisfoldercreatingadatacontainerorResultSet.AllsubsequentactionsfortherunswithinaResultSet(calibrating,reviewing,reprocessing,etc.)usethefilesintheResultSet.EachsequencecreatesaResultSetwithamethodforthesequenceasawhole.Eachdatafilecontainsacopyofthemethodusedtocreatetherun:DA.M(savedafterautomateddataanalysis).11ResultSetsSequenceMethod(CopyofMasterMethod)DataFilesBatchFileSequenceFile(CopyofSequenceTemplate)AResultSetisacompletepackageforexaminingandprocessinganalysisresults.LogbookReportTemplate(.rdl)ResultsFile12DataFileContentsDAMethodSignalLogbook13ExploringDataintheChemStationExplorer13DataPathResultSetDataFolderSingleRunsinFolder14AgandaOpenLABCDS软件使用–数据重新处理15DataAnalysisWorkflowsReprocessMode–Onlyavailablewhenworkingwithresultsets.–Usesthesequenceenginetoprocessdatafiles.RecalculateMode–Worksonanydatainthenavigationtable–doesnotneedtobeinaresultset.–Resultscanbecalculatedwitheithertheloadedmethodortheindividualdatafile’smethod(DA.M).ReviewView–Noloadingofmethodordatafile.–Choosefileandreporttemplatetoview.–Basedoncurrentresults(storedinACAMLfile).–OnlyavailableifyouhaveconfiguredIntelligentReporting.16WhatisaResultSet?Auser-assembledresultsetcanalsobecreatedfromdatafilesinthenavigationtable.AresultsetwillbeautomaticallygeneratedforanysequencesthatarerunifUniquefoldercreationissettoONinthePreferencesdialogbox.17Onlyavailablewhenaresultsetisloadedintothenavigationtable.Recalibratewithdifferentorchangedmethod.Calculatenewresultsusingdifferentorchangedmethod.Usesthesequenceenginetoreprocessdata.Followsorderasinthesequencetable.SequenceReprocessingReprocessingtoolbar.Reprocessmodeselectiontool.18LoadandReviewSequenceDataSubdirectoryspecifiedinSequenceParameters.Sequenceresultset(folder).FindandloadsequencedataintoNavigationTableDouble-clickonfilerowtoloaddatafile.TypeofrunSingleRunFromanold-stylesequenceFromaresultsetFromauserassembledresultsetReprocessmode19ReprocesstheSequenceReprocesswhenready.20SequenceReprocessingBluecolorindicatesreprocessingmode.Indicatescurrentsamplereprocessing.StopReprocessing21UpdateMethodsIfdesired,updatetheoriginalMastermethodwiththemodificationsmadetotheSequencemethod.Thesechangeswillthenbeavailablewhennewsequencesareacquired.Alternately,anewMasterMethodcanbecreated.UpdatestotheMastermethodcanoccurautomaticallyviatheSequenceParametersdialogbox.Contextmenuavailable.22UpdateMethodsDraganddropfromMasterMethodsfoldertoresultsetorusearrowbutton.SequenceMethodsthathavebeenmodifiedcanupdatecorrespondingMasterMethodsviathisinterface.UsetheUpdateMethodsdialogtoeasilyviewsequenceandmastermethods•MethodscommontobothresultfileandMasterMethodfolderareshowninbold.•Methodsprefacedbyan(R)areread-only.•Thecurrentmethodisinitalics.23ReprocessingwithDifferentMethod1.Choosemenuitem2.Selectnewreprocessingmethod.3.Reprocessingbeginsafterchoosingthenewmethodandfollowstheorderinthesequencetable.24ReprocessingwithDifferentMethod4.TheSequencetablehasbeenupdatedwithdifferentmethodandcanbesavedasanewtemplate.5.Thenewreprocessingmethodisaddedtotheresultset.25SequenceReprocessingwithManualIntegration(1)PerformManualIntegration.(2)SaveManualEventstoDataFile.(3)ManualEventsMarkedinTable(4)Reprocess26SequenceReprocessingwithManualIntegrationReprocessingusesSequenceMethodManualIntegrationisstoredwithdatafile–notmethodReportindicatesManualIntegration27PartialSequenceReprocessinginDataAnalysis28MethodAuditTrail29AgandaOpenLABCDS软件使用–结果集30UserAssembledResultSetStep1–CleartheNav