傅立叶变换红外光谱技术在润滑油行业的应用

20112Feb.2011LUBRICATINGOIL261Vo.l26,No.1ANALYSIS&EVALUATION:1002-3119(2011)01-0044-05,,,(,215433):,,(FTIR):;;;;;:TE626.3:AApplicationsofFTIRinLubricantIndustryHUJing,LIJian,YANGChun-hua,SANGuo-wen(PetroChinaHuadongLubricantBlendingPlant,Taicang215433,China)Abstract:Theinfraredspectroscopyanalysistechnologyisahighlyeffectiveandfastmodernanalysistechnology.Inrecentyears,ithasbeenappliedmoreandmorewidelyinlubricantindustry.Inthispaper,theapplicationsofFTIRinlubricantarebrieflydescribed,includingthequalityanalysisoflubricatingoilanditsadditive,thedeterminationofadditivecontentinlubr-icatingoi,lsolvingoilqualityproblemsandthequalitymonitoringofin-uselubricatingoi,landsoon.Keywords:infraredspectroscopy;lubricatingoi;ladditive;qualitymonitoring;analysis;application0,(FTIR),,,,,;,,,;,,,,,,,,,,1FTIR,,,,,1.45ANALYSIS&EVALUATION,,,,,2000,[1],FTIR,,,,,,SH/T02512007,[2]NicoletMagna750,ATR,860cm-1(CO32-),SH/T0251,5%,(:),,,,,,10min,2FTIR,,,,,,,[3]ICP[4],ZDDP,ZDDP,,,,ICP,,,,,1995,[5]ZDDPE644,667cm-1ZDDP,1706cm-1E644,,ZDDPE644,7%5%1999,[6]PE)FTIRPE/Quant0,SE15W-40SE/CD15W-30CD15W-40CC15W-300.2%~90%,10%2000,[7]PEFTIR1725X/Quant0ZDDPZDDP(T202):0.5%1.0%1.5%2.0%2.5%5,:150SN85%,OCP15%ZDDP,,/Quant0,,ZDDP5%2003,[8],IFS66V,,T5010.1%~1.0%,,3650cm-1,,,3650cm-1,,,46201126ANALYSIS&EVALUATIONT501,,,2007,[9],,,43FTIR,,,;;,,1999,[10-11]PE1725X,,100e,8100e,3.37%3.12%,,,,,,2008,[12]FTIR370,(,TFA),,,,,5%4FTIR,,,,,,,,,;,,,,,,,,,,,,,2008,[13],,,ICP)AES,FT-IR,,,,,,,,,,,,,,5FTIR,,,1.47ANALYSIS&EVALUATION;,,,,,,,(ASTME2412-04),,1994,[14],2000,[15],,CF-415W-40,6000km,,,,2001,[16],,2003,[17]NicoletAVA-TAR360,,,2006,[18],T501,T5012008,[19]A370,CF-415W-40,,CF-415W-40,,2009,[20],,5%,[21],,,(GB/T260)[22]FTIRAvatar360ML,,MLFTIRAvatar360FTIR,,,6(1),,,,(2),,,(3),,,(4),,48201126ANALYSIS&EVALUATION(5),,:[1],,,.[J].,2000,10(4):38-39.[2],,.[J].,2007,22(2):49-53.[3],.[J].,1995(4):20-23.[4],,.ICP-AES[J].,2007,22(5):55-58.[5].[J].,1995(3):36-37.[6],.[J].,1999,19(2):189-190.[7],,.FTIRZDDP[J].,2000(5):54-55.[8],.T501[J].,2003(4):20-23.[9].[J].,2007,34(2):38-40.[10],,.100e[J].,1999,16(4):388-390.[11],,,.[J].,1999,19(4):229-561.[12],,,.[J].,2008,33(9):65-66.[13],,,.[J].,2008,27(4):71-72.[14].[J].,1994,9(6):28-33.[15],,.[J].,2000(4):31-33.[16].[J].,2001(2):90-91.[17].[J].,2003,18(1):44-46.[18],.[J].,2006,23(4):20-22.[19].[J].,2008,23(3):57-59.[20],,.FTIR[J].,2009,25(2):46-49.[21],,.[J].,2009,34(9):102-104.[22],,.FTIR[J].,2009,34(7):84-87.:2010-07-01:(1981-),,,2006,ICIS第15届基础油和润滑油会议将于2011年在英国举行ICIS第15届世界基础油和润滑油会议将于2011年2月24~25日在伦敦Lancaster召开会议主要内容包括:全球基础油和润滑油市场的最新发展趋势和市场驱动力;全球润滑油新兴市场的环境;生物燃油如何影响润滑油行业等会议将邀请润滑油基础油及相关行业人员参加,其中IpirangaLukoilChevronNesteIveco和GeneralMotors将在本次会议上做相关内容报告