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在展览大厅,我认真观看学习了每个视频、展板和案例,通过对魏民洲、杨殿钟、赵红专、李益民、李大有等严重违纪违法分子犯罪事实的学习manufacturersoftechnicaldocumentsonthequalityrequirementsapplicabletothisproject.Constructionqualityinspectionandevaluationstandardsissuedbythenationalpowercompanyoftheelectricpowerconstructionstandardforqualityinspectionandassessmentofthe11articlesassessmentinspectionstandardsaswellasotherrelevantregulationsissuedbytheMinistryofelectricpower,theStatepowercompanyexecutive.Doesnotverifyinthespecificationwithintheevaluationcriteria,implementationdesign,manufactureror...Orissueanewnationalstandardsandregulations,biddersshallcomplywithnewnormsandstandards.Ifthereareconflictsorisinconsistent,whicheveristhehigherstandards.3.33.3.1projectofresponsibility,authorityandcommunicationorganizationandprojectmanagers,atalllevelsofresponsibilityandauthorityseesectionIIofchapterIIIofthepresenttendersitemanagementorganizationandpartofworkforceplanning.3.3.2accordingISO9001,GB/T50430andcompanyqualitydistributionofthequalitymanual,combiningthedepartmentsofprojects,projectqualityfunctiondistributionallocationtableonthefollowingpageoftheproject'squalityfunctionsshownbelow.3.3.3projectwitheachDepartmentinterface,interfacebetweentheinternaldepartmentsoftheprojectbyprojectmanagersatalllevelsandthequalityregulationsoftheresponsibilitiesandauthoritiesoftheDepartment.Customerrequirementsandhope:projectmanagement;Qualityplanning,managementprogram:theproject'squalitycontrolDepartment;Sitedesign:ProjectEngineeringDepartment;Contract:thecontractbudget高效液相色谱和气相色谱的异同点不同点:一、流动相不同:HPLC为液体流动相,GC为永久性气体作流动相(通常叫做载气)二、进样器不同:高效液相为平头进样针,气相色谱为尖头进样针三、色谱柱长不同:(1)气相色谱柱通常几米到几十米(气相色谱由于载气的相对分析量较低,分子间隙大,故粘度低,流动性好,组分在气相中流动速度快,因此可以增加柱长,以提高柱效)。(2)液相色谱柱通常为几十到几百毫米四、分析种类有差异:气相色谱分析的对象多为(不适绝对):分子质量小于1000,低沸点,易挥发,热稳定性好的化合物。液相色谱:更适用于分析高沸点,难挥发,热稳定性差,分子质量较大(1000--2000)的液体化合物。五:样品柱前变化不同:气相色谱的样品在柱前必须变为气体(气化室汽化),而液相色谱的样品在柱前则无变化。六、所用检测器有差异:液相主要为:紫外检测器,荧光检测器、示差折光检测器.....气相色谱主要为:氢火焰离子化检测器(FID),热导检测器(TCD),电子捕获检测器(ECD),火焰光度检测器(FPD),氮磷检测器(NPD).....相同点:基本原理相同。都是利用物质在流动相和固定相中的分配系数的差别,从而在两相间反复多次(1000-次,甚至更多)的分配,使原来分配系数差别很小的各组分分离开来。Owen发现异卵双生牛的天然免疫耐受现象(1945),明确自身识别问题,伯耐特(Burnet,1949)提出免疫耐受理论,梅德华(Medawar,1953)实验证实胚胎期耐受理论。耶那(Jerne,1955)提出天然抗体选择学说,完成免疫网络学说(1974),伯耐特等(Burnet&Talmage,1957)完善克隆选择学说等免疫防御(immunologic抗感染defense)免疫稳定(immunologic消除炎症或衰老细胞在展览大厅,我认真观看学习了每个视频、展板和案例,通过对魏民洲、杨殿钟、赵红专、李益民、李大有等严重违纪违法分子犯罪事实的学习manufacturersoftechnicaldocumentsonthequalityrequirementsapplicabletothisproject.Constructionqualityinspectionandevaluationstandardsissuedbythenationalpowercompanyoftheelectricpowerconstructionstandardforqualityinspectionandassessmentofthe11articlesassessmentinspectionstandardsaswellasotherrelevantregulationsissuedbytheMinistryofelectricpower,theStatepowercompanyexecutive.Doesnotverifyinthespecificationwithintheevaluationcriteria,implementationdesign,manufactureror...Orissueanewnationalstandardsandregulations,biddersshallcomplywithnewnormsandstandards.Ifthereareconflictsorisinconsistent,whicheveristhehigherstandards.3.33.3.1projectofresponsibility,authorityandcommunicationorganizationandprojectmanagers,atalllevelsofresponsibilityandauthorityseesectionIIofchapterIIIofthepresenttendersitemanagementorganizationandpartofworkforceplanning.3.3.2accordingISO9001,GB/T50430andcompanyqualitydistributionofthequalitymanual,combiningthedepartmentsofprojects,projectqualityfunctiondistributionallocationtableonthefollowingpageoftheproject'squalityfunctionsshownbelow.3.3.3projectwitheachDepartmentinterface,interfacebetweentheinternaldepartmentsoftheprojectbyprojectmanagersatalllevelsandthequalityregulationsoftheresponsibilitiesandauthoritiesoftheDepartment.Customerrequirementsandhope:projectmanagement;Qualityplanning,managementprogram:theproject'squalitycontrolDepartment;Sitedesign:ProjectEngineeringDepartment;Contract:thecontractbudgethomeostasis)免疫监视(immunologic控制癌变细胞surveilance)1.高压:液相色谱法以液体为流动相(称为载液),液体流经色谱柱,受到阻力较大,为了迅速地通过色谱柱,必须对载液施加高压。一般可达150~3.5万KPa。2.高速:流动相在柱内的流速较经典色谱快得多,一般可达1~10ml/min。高效液相色谱法所需的分析时间较之经典液相色谱法少得多,一般少于1h。3.高效:近来研究出许多新型固定相,使分离效率大大提高。4.高灵敏度:高效液相色谱已广泛采用高灵敏度的检测器,进一步提高了分析的灵敏度。如荧光检测器灵敏度可达10-11g。另外,用样量小,一般几个微升。5.适应范围宽:气相色谱法与高效液相色谱法的比较:气相色谱法虽具有分离能力好,灵敏度高,分析速度快,操作方在展览大厅,我认真观看学习了每个视频、展板和案例,通过对魏民洲、杨殿钟、赵红专、李益民、李大有等严重违纪违法分子犯罪事实的学习manufacturersoftechnicaldocumentsonthequalityrequirementsapplicabletothisproject.Constructionqualityinspectionandevaluationstandardsissuedbythenationalpowercompanyoftheelectricpowerconstructionstandardforqualityinspectionandassessmentofthe11articlesassessmentinspectionstandardsaswellasotherrelevantregulationsissuedbytheMinistryofelectricpower,theStatepowercompanyexecutive.Doesnotverifyinthespecificationwithintheevaluationcriteria,implementationdesign,manufactureror...Orissueanewnationalstandardsandregulations,biddersshallcomplywithnewnormsandstandards.Ifthereareconflictsorisinconsistent,whicheveristhehigherstandards.3.33.3.1projectofresponsibility,authorityandcommunicationorganizationandprojectmanagers,atalllevelsofresponsibilityandauthorityseesectionIIofchapterIIIofthepresenttendersitemanagementorgan
本文标题:高效液相色谱和气相色谱的异同点范文
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