Mastersizer2000分析报告解析

Mastersizer2000舒霞1,吴玉程1,陶庆秀2,程继贵1,夏永红1(1.合肥工业大学材料科学与工程学院,安徽合肥230009;2.合肥工业大学实验室与设备处,安徽合肥230009):Mastersizer2000,,:;;Mastersizer2000:TH873:B:10024956(2011)02003705AnanalysisonreportofMastersizer2000laserparticlesizeanalyzerShuXia1,WuYucheng1,TaoQingxiu2,ChengJigui1,XiaYonghong1(1.SchoolofMaterialScienceandEngineering,HefeiUniversityofTechnology,Hefei230009,China;2.DepartmentofLaboratoryandEquipment,HefeiUniversityofTechnology,Hefei230009,China)Abstract:BasedontheparticlesizemeasurementpracticeandtheexamplesofMastersizer2000laserparticlesizeanalyzer,thecolumncontentandparametercharacteristicsofthetypicalparticleanalysisreportaredeeplyanalyzed,hopingtoprovidesomeusefulreferencesattheaspectoftheapplicationoflaserparticlesizeanalyzerandresultsanalysis.Keywords:particlesizeanalysis;laserparticlesizeanalyzer;Mastersizer2000:20100406:20100726:(1971),,,,,Email:[e-mail]:(1962),,,,,,.2003Mastersizer2000,,,,1,,,Mastersizer2000(Mie),,Mie,,(),(),()2r,,=4/3r3:50mm25mm10mm,,,30mm,30mmD10D50D90[13]22.111:SOP,SOPMastersizer2000ISSN1002-4956CN11-2034/TExperimentalTechnologyandManagement28220112Vol.28No.2Feb.2011:SOPSOP,SOP,,,,,SOPMeasurement,,2.222,()(1),(2.610),,1.0,0.1,1m0,1m0.001,,,0.1,Mastersizer2000,,Mastersizer2000(),,,,,,,[45]:,,,,,,1131d0.1d0.5d0.9()1.550.010.0650.1220.2247.28210.0811.60.010.0690.130.5843.6288.28521.620.010.0650.1230.6243.5977.91731.650.010.0640.1230.7052.9767.14241.70.010.0650.1261.1252.565.85451.80.010.0670.1451.431.8023.34562.00.010.2490.9042.4880.8151.14272.20.010.4090.972.4621.0061.322111:,(1.55),,;,;2,1%,;2.2,22()SEM(3)(1),382()3SEM(2000)(2),,1%1%,,(5m),3%,,(,)(3),(4),;,,10%~20%,,,(5)Hydro2000MU(A),,,,(6)Mastersizer20000.02m2000m(7),Mastersizer2000,Mastersizer,[6]:280,2,,d5052.81m,(27053m),,,452d0.1d0.910%90%2d0.1d0.5d0.9SiC2.610.535.35852.7578.4960.471SiC2.610.535.41752.84878.6260.474SiC2.610.535.40952.83378.6140.474SiC2.610.535.39552.8178.5790.4732.333(1),BeerLambert(),,,(2),,=d0.9-d0.1d0.5(3),d[4,3]d0.539,:Mastersizer200045(4),,,BET[78]D[3,2]()D[4,3][9]3123,,D[1,0]=dn=1+2+33=2,nD[1,0],,,D[2,0]=d2n12+22+323=2.16,,,D[3,0]=d3n=13+23+333=2.29,,,,D[3,2]()D[4,3],D[4,3],D[3,2],D[3,2]D[4,3]:D[3,2]=d3d2=13+23+3312+22+32=2.57D[4,3]=d4d3=14+24+3413+23+33=2.72,(),,,?Mastersizer:1:,,350,1kg2kgD[1,0],D[4,3]2:,,,,,2.444,3d0.1d0.5d0.9,md0.5,,50%,50%d0.5,,,,,,,mMastersizer2000,,,,15%,,,(),0.24~0.275m,40,,3:%%%,(origin),,2.555,,,Hydro2000MU(A),,,3,,:文中图3由合肥工业大学材料学院朱继平老师提供感谢马尔文仪器上海思百吉仪器系统有限公司提供的技术支持(References)[1],,,.[J].,2002,32(4):608614.[2].[J].,2000(1):5859.[3]JonesRM.ISO13320,:[EB/OL].[20100115].[4],,,.[J].,2002,8(5):2830.[5],.[J].,2002,25(5):5557.[6],,.[J].,2001,19(3):449454.[7].ISO92771995BET[J].,1996,6(2):3843.[8],,,.BET[J].,2001,24(1):78.[9]RaweA.Basicprinciplesofparticlesizeanalysis[EB/OL].(2006).(上接第36页),,7FRP75FRP,:(1);(2),;(3)FRP(References)[1],.[J].,2002,35(3):1319.[2],,.[J].FRP,2002(3):105110.[3],,,.FRP[J].,2002,32(5):7567.[4],,.[J].,2002,28(3):1921.[5],,.[J].,2007,32(6):1418.[6].GB/T500812002[S].:,2002.[7].CECS1462003[S].:,2003.[8],.[M].:,2003.41,:Mastersizer2000