EPA-8270-气相色谱质谱法分析半挥发性有机物(中文版)

方法8270D气质联用仪测试半挥发性有机化合物技术翻译：刘金云mail:[e-mail]1.0范围及应用1.1方法8270用于测定多种类型的固体废弃物基体、土壤、空气取样媒介及水样制备的萃取物中的半挥发性有机化合物的浓度.直接注入样品的使用范围是有限的.以下的化合物可以通过此方法测试.合适的前置处理技术b化合物CAS编号a351035203540/354135503580苊83-32-9ⅩⅩⅩⅩⅩ苊嵌戊烯208-96-8ⅩⅩⅩⅩⅩ乙酰苯98-86-2ⅩNDNDNDⅩ2-乙酰氨基芴53-96-3ⅩNDNDNDⅩ1-乙酰基-2-硫脲591-08-2LRNDNDNDLR艾氏剂309-00-2ⅩⅩⅩⅩⅩ氨基蒽醌117-79-3ⅩNDNDNDⅩ氨基偶氮苯60-09-3ⅩNDNDNDⅩ4-氨基联苯92-67-1ⅩNDNDNDⅩ3-氨基-9-乙基咔唑132-32-1ⅩⅩNDNDND敌菌灵101-05-3ⅩNDNDNDⅩ苯胺62-53-3ⅩⅩNDⅩⅩ茴香胺90-04-0ⅩNDNDNDⅩ蒽120-12-7ⅩⅩⅩⅩⅩ异黄樟140-57-8HS（43）NDNDNDⅩ氯化联二苯树脂101612674-11-2ⅩⅩⅩⅩⅩ氯化联二苯树脂122111104-28-2ⅩⅩⅩⅩⅩ氯化联二苯树脂123211141-16-5ⅩⅩⅩⅩⅩ氯化联二苯树脂124253469-21-9ⅩⅩⅩⅩⅩ氯化联二苯树脂124812672-29-6ⅩⅩⅩⅩⅩ氯化联二苯树脂125411097-69-1ⅩⅩⅩⅩⅩ氯化联二苯树脂126011096-82-5ⅩⅩⅩⅩⅩ谷硫磷86-50-0HS（62）NDNDNDⅩ氯炔草灵101-27-9LRNDNDNDLR联苯胺92-87-5CPCPCPCPCP苯甲酸65-85-0XXNDXX合适的前置处理技术b化合物CAS编号a351035203540/354135503580苯并蒽56-55-3ⅩⅩⅩⅩⅩ苯并（b）荧蒽205-99-2ⅩⅩⅩⅩⅩ苯并（k）荧蒽207-08-9ⅩⅩⅩⅩⅩ苯并（g,h,i）茈191-24-2ⅩⅩⅩⅩⅩ苯并（a）芘50-32-8ⅩⅩⅩⅩⅩp-苯醌106-51-4OENDNDNDX苯甲醇100-51-6ⅩⅩNDⅩⅩα-六氯化苯319-84-6ⅩⅩⅩⅩⅩβ-六氯化苯319-85-7ⅩⅩⅩⅩⅩδ-六氯化苯319-86-8ⅩⅩⅩⅩⅩγ-六氯化苯（林旦）58-89-9ⅩⅩⅩⅩⅩ双（2-氯乙氧基）甲烷111-91-1ⅩⅩⅩⅩⅩ双(2-氯乙基）醚111-44-4ⅩⅩⅩⅩⅩ双（2-氯异丙基）醚108-60-1ⅩⅩⅩⅩⅩ双（2-氯乙基己基）邻苯二甲酸酯117-81-7ⅩⅩⅩⅩⅩ4-溴苯基苯醚101-55-3ⅩⅩⅩⅩⅩ溴苯腈1689-84-5ⅩNDNDNDⅩ邻苯二甲酸丁基·苄基酯85-68-7ⅩⅩⅩⅩⅩ敌菌丹2425-06-1HS（55）NDNDNDⅩ克菌丹133-06-2HS（40）NDNDNDⅩ甲萘威63-25-2ⅩNDNDNDⅩ呋喃丹1563-66-2ⅩNDNDNDⅩ二硫磷786-19-6ⅩNDNDNDⅩ氯丹（NOS）57-74-9ⅩⅩⅩⅩⅩ毒虫威470-90-6ⅩNDNDNDⅩ4-氯苯胺106-47-8ⅩNDNDNDⅩ乙酯杀螨醇510-15-6ⅩNDNDNDⅩ对氯邻氨基甲苯95-79-4ⅩNDNDNDⅩ4-氯-3-甲苯酚59-50-7ⅩⅩⅩⅩⅩ3-（氯甲苯）吡啶盐6959-48-4ⅩNDNDNDⅩ酸盐1-氯代萘90-13-1ⅩⅩⅩⅩⅩ2-氯代萘91-58-7ⅩⅩⅩⅩⅩ2-氯苯酚95-57-8ⅩⅩⅩⅩⅩ4-氯-1,2-苯二胺95-83-0ⅩⅩNDNDND4-氯-1,3-苯二胺5131-60-2ⅩⅩNDNDND4-氯苯基苯醚7005-72-3ⅩⅩⅩⅩⅩ合适的前置处理技术b化合物CAS编号a351035203540/3541355035801,2-苯并菲218-01-9ⅩⅩⅩⅩⅩ香豆磷56-72-4ⅩNDNDNDⅩ甲酚定120-71-8ⅩNDNDNDⅩ丁烯磷7700-17-6ⅩNDNDNDⅩ2-环己烯-4,6-二硝基-苯酚131-89-5ⅩNDNDNDLR4,4-DDD72-54-8ⅩⅩⅩⅩⅩ4,4-DDE72-55-9ⅩⅩⅩⅩⅩ4,4-DDT50-29-3ⅩⅩⅩⅩXO-异内吸磷298-03-3HS（68）NDNDNDⅩS-异内吸磷126-75-0ⅩNDNDNDⅩ燕麦敌（顺式或反式）2303-16-4ⅩNDNDNDⅩ2,4-二氨基甲苯95-80-7DC,0E（42）NDNDNDⅩ二苯并（a,j）吖啶224-42-0ⅩNDNDNDⅩ二苯并（a,h）蒽53-70-3ⅩⅩⅩⅩⅩ二苯并呋喃132-64-9ⅩⅩNDⅩⅩ二苯并（a,e）芘192-65-4NDNDNDNDⅩ1，2-溴-3-氯丙烷96-12-8ⅩⅩNDNDND苯二甲酸-n-二丁酯84-74-2ⅩⅩⅩⅩⅩ二氯萘醌117-80-6OENDNDNDⅩ1,2-二氯代苯95-50-1ⅩⅩⅩⅩⅩ1,3-二氯代苯541-73-1ⅩⅩⅩⅩⅩ1,4-二氯代苯106-46-7ⅩⅩⅩⅩⅩ3,3-二氯联苯胺91-94-1ⅩⅩⅩⅩⅩ2,4-二氯苯酚120-83-2ⅩⅩⅩⅩⅩ2,6-二氯苯酚87-65-0ⅩNDNDNDⅩ敌敌畏62-73-7ⅩNDNDNDⅩ百治磷141-66-2ⅩNDNDNDⅩ狄氏剂60-57-1ⅩⅩⅩⅩⅩ酞酸二乙酯84-66-2ⅩⅩⅩⅩⅩ乙烯雌酚56-53-1AW，NDNDNDⅩ0S（67）硫酸二乙酯64-67-5LRNDNDNDLR乐果60-51-5HE，NDNDNDⅩHS（31）3，3`-二甲氨基联苯氨119-90-4ⅩNDNDNDLR二甲氨基偶氮苯60-11-7ⅩNDNDNDX7,12甲基苯并（a）蒽57-97-6CP（45）NDNDNDCP合适的前置处理技术b化合物CAS编号a351035203540/3541355035803,3`-二甲基联苯胺119-93-7ⅩNDNDNDⅩα,α-二甲基苯乙胺122-09-8NDNDNDNDⅩ2,4-二甲苯酚105-67-9ⅩⅩⅩⅩⅩ苯二甲酸二甲酯131-11-3ⅩⅩⅩⅩⅩ1,2-二硝基苯528-29-0ⅩNDNDNDX1,3-二硝基苯99-65-0ⅩNDNDNDⅩ1,4二硝基苯100-25-4HE（14）NDNDNDⅩ4,6-二硝基-2-甲酚534-52-1ⅩⅩⅩⅩⅩ2,4-二硝基苯酚51-28-5ⅩⅩⅩⅩⅩ2,4-二硝基甲苯121-14-2ⅩⅩⅩⅩⅩ2,6二硝基甲苯606-20-2ⅩⅩⅩⅩⅩ敌螨普39300-45-3CP，HSNDNDNDCP（28）二硝丁酚88-85-7ⅩNDNDNDⅩ二苯胺122-39-4ⅩⅩXⅩⅩ苯妥英57-41-0XNDNDNDⅩ1,2-二苯肼122-66-7ⅩⅩⅩⅩⅩ磷酸-n-二辛酯117-84-0ⅩⅩⅩⅩⅩ乙拌磷298-04-4XNDNDNDⅩ硫丹Ⅰ959-98-8ⅩⅩⅩⅩⅩ硫丹Ⅱ33213-65-9ⅩⅩⅩⅩⅩ硫酸硫丹1031-07-8ⅩⅩⅩⅩⅩ异狄氏剂72-20-8ⅩⅩⅩⅩⅩ异狄氏剂醛7421-93-4ⅩⅩⅩⅩⅩ异狄氏剂酮53494-70-5ⅩXNDXⅩ苯硫磷2104-64-5ⅩNDNDNDⅩ乙硫磷563-12-2ⅩNDNDNDⅩ氨基甲酸乙酯51-79-6DC（28）NDNDNDⅩ乙基甲磺酸62-50-0ⅩNDNDNDⅩ氨磺磷52-85-7ⅩNDNDNDⅩ丰索磷115-90-2ⅩNDNDNDⅩ倍硫磷55-38-9ⅩNDNDNDⅩ氯氟灵33245-39-5ⅩNDNDNDⅩ荧蒽206-44-0ⅩⅩⅩⅩⅩ芴86-73-7ⅩⅩⅩⅩⅩ2-氟（代）联苯321-60-8ⅩⅩⅩⅩⅩ2-氟（代）苯酚367-12-4ⅩⅩⅩⅩⅩ合适的前置处理技术b化合物CAS编号a351035203540/354135503580七氯化茚76-44-8XXXXX七氯环氧化物1024-57-3XXXXX六氯化苯118-74-1XXXXX六氯丁二烯87-68-3XXXXX六氯环戊二烯77-47-4XXXXX六氯乙烷67-72-1XXXXX六氯酚70-30-4AW，NDNDNDCPCP（62）六氯丙烯1888-71-7XNDNDNDX六甲基磷酸三酰胺680-31-9XNDNDNDX对苯二酚123-31-9NDNDNDNDX茚并（1，2，3-cd）芘193-39-5XXXXX异艾氏剂465-73-6XNDNDNDX异佛尔酮78-59-1XXXXX异黄樟素120-58-1DC（46）NDNDNDX十氯酮143-50-0XNDNDNDX溴苯磷21609-90-5XNDNDNDX马拉硫磷121-75-5HS（5）NDNDNDX顺丁烯二酸酐108-31-6HENDNDNDX炔雌醇甲醚72-33-3XNDNDNDX噻吩甲吡胺91-80-5XNDNDNDX甲氧氯72-43-5XNDNDNDX甲基胆蒽56-49-5XNDNDNDX4,4`-亚甲基双101-14-4OE，OSNDNDNDLR（-2氯苯胺）（0）4,4`-亚甲基双101-61-1XXNDNDND（N,N-二甲基-苯胺）甲基甲磺酸66-27-3XNDNDNDX2-甲基萘91-57-6XXNDXX甲基对硫磷298-00-0XNDNDNDX2-甲苯酚95-48-7XNDNDNDX3-甲苯酚108-39-4XNDNDNDX4-甲苯酚106-44-5XNDNDNDX速灭磷7786-34-7XNDNDNDX兹克威315-18-4HE，HSNDNDNDX（68）灭蚁灵2385-85-5XNDNDNDX久效磷6923-22-4HENDNDNDX合适的前置处理技术b化合物CAS编号a351035203540/354135503580二溴磷300-76-5ⅩNDNDNDⅩ萘91-20-3ⅩⅩⅩⅩⅩ萘醌130-15-4ⅩNDNDNDⅩ1-萘胺134-32-7OS（44）NDNDNDⅩ2-萘胺91-59-8ⅩNDNDNDⅩ烟碱54-11-5DE（67）NDNDNDX5-硝基苊602-87-9ⅩNDNDNDⅩ2-硝基苯胺88-74-4ⅩⅩNDⅩⅩ3-硝基苯胺99-09-2ⅩⅩNDⅩⅩ4-硝基苯胺100-01-6ⅩⅩNDⅩⅩ2-甲氧基-5-硝基苯胺99-59-2ⅩNDNDNDⅩ硝基苯98-95-3ⅩⅩⅩⅩⅩ4-硝基联苯92-93-3ⅩNDNDNDⅩ除草醚1836-75-5ⅩNDNDNDⅩ2-硝基苯酚88-75-5ⅩⅩⅩⅩⅩ4-硝基苯酚100-02-7ⅩⅩⅩⅩⅩ5-硝基-2-甲苯胺99-55-8ⅩXNDNDⅩ硝基硅啉-1-氧化物56-57-5ⅩNDNDNDⅩN-亚硝基二丁胺924-16-3XNDNDNDⅩN-亚硝基二乙胺55-18-5XNDNDNDⅩN-亚硝基二甲胺62-75-9ⅩXXXⅩN-亚硝基甲基乙胺10595-95-6ⅩNDNDNDⅩN-亚硝基二苯胺86-30-6ⅩXXXⅩN-亚硝基二丙胺621-64-7ⅩⅩⅩⅩⅩ亚硝基吗啉59-89-2NDNDNDNDⅩN-亚硝基呱啶100-75-4ⅩNDNDNDⅩ亚硝基吡咯烷930-55-2ⅩNDNDNDⅩ八甲基焦磷酰胺152-16-9LRNDNDNDLR4,4`-羟基二苯胺101-80-4ⅩNDNDNDⅩ对硫磷56-38-2ⅩXNDNDⅩ五氯苯608-93-5XNDNDNDX五氯硝基苯82-68-8ⅩNDNDNDⅩ五氯苯酚87-86-5ⅩⅩⅩⅩⅩ非那西丁62-44-2ⅩNDNDNDⅩ菲85-01-8ⅩⅩXXX菲巴比妥50-06-6ⅩNDNDNDⅩ苯酚108-95-2DC（28）ⅩⅩⅩⅩ合适的前置处理技术b化合物CAS编号a351035203540/3541355035801,4-苯二胺106-50-3ⅩNDNDNDⅩ甲拌磷298-02-2ⅩⅩⅩⅩⅩ伏杀硫磷2310-17-0HS（65）NDNDNDⅩ亚胺硫磷732-11-6HS（15）NDNDNDⅩ磷胺13171-21-6HE（63）NDNDNDⅩ酞酐85-44-9CP,HE(1)NDNDNDCP2-皮考啉（2-甲基吡啶）109-06-8ⅩXNDNDND胡椒基亚砜120-62-7ⅩNDNDNDⅩ拿草特23950-58-5