4-氯乙酰乙酸乙酯的合成

第30卷第6期辽宁化工Vol.30,No.62001年6月LiaoningChemicalIndustryJune,20014-翟煜翥(,110044):4-:4-;;:TQ225.24:A:10040935(2001)0602400114-,,,,,,,,,,,,233.11000ml3.23.3(1)500ml,,150g,0.3g,0.6g,,0e,0e()(2),,,40g/h,3e,,(3),,,100ml,,,1h(4)15%pH=7~8,,,,0.5g,,4-230g(5),98%4(1),(242)收稿日期:2001204205作者简介:翟煜翥(1969-),男,工程师,2,5%,2,,,,,2A-1A-5A-6A-7A-801.01.52.03.03.02.01.51.003.03.03.03.03.0/(kJ#m-2)4.738.4916.8522.027.0/=4.2/2.1,30%1,2,1,,4(1)1;(2)[1]..,1988[2],..(),1989,(1):59-62StudyonTougheningofUnsaturatedPolyesterResinZHANGPeng2fei,LUBo,LIMei(1.LiaoyangAcademyofPetrolchemcalTechnology,Liaoyang111000,China;2.ShenyangInstituteofChemicalTechnologyShenyang110021,China)Abstract:Synthesisofunsaturatedpolyesterresinwithdifferentmoleratioofadipicacidtodiethyleneglycolandeffectsoftougheningwerestudied.Theresultsshowedthattheeffectoftougheningissimilarbyadipicacidtodiethyleneglycol,buttheeffectoftougheningisdistinctbyadipicacidanddiethyleneglycol.Keywords:Unsaturatedpolyesterresin;Toughening;Condensationpolymerization(240),HCl,HCl,(2),,4h,,-5e(3),(4),,,,Synthesisof4-ChloracetylAcetidinZAIYu2zhuAbstract:Synthesisandapplicationof4-chloracetylacetidinwereintroduced.Keywords:4-Chloracetylacetidin;Synthesis;Alcohol242辽宁化工2001年6月