DB13T 1081.1-2009 食品用包装材料及制品 塑料 第1部分：化学物质迁移量和含量的测定

ICS67.250X08DB13JTrpJDB13/T1081.1-20091Foodpackagingmaterialsandarticles-Plastics-Guidetotestmethodsforthespecificmigrationofchemicalsubstancesfromplasticsmaterialandarticletofoodsimulantsandthedeterminationofsubstancesinplastics2009-05-272009-06-11dDB13/T1081.1-2009.............................................................................IV112131434.134.244.344.444.5testmediumsubstiitefattests)....................44.6alternativefattest...................................44.7.......................................................44.844.94545.145.255.3Alternativefattests.................................................55.45666.166.266.3testmedium...............................................................66.46U0UnO90qqUnb1Jd11111J117¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤7.17.2¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤7.37.47.5¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤8alternative8.1¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤8.2¡¤8.3Alternativefattest99.1¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤9.2¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤9.39.4¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤¡¤DB131081.1-200910............................................................................1610.1..........................................................................1610.2......................................................1610.3..................................................1710.4TypeAMark2.............................................1710.51710.61710.71810.81810.91810.101810.111810.121810.1318111911.11911.2191219131913.11913.22013.3QA2013.42113.5..................................................................2114.............................................................2115...........................2115.12115.22115.321.42215.52215.622162316.12316.22316.32316.4.....................................................2316.52316.62317................................................2317.123182518.1....................25DB13/T1081.1-200918.22518.32518.42518.525A.........................................27B..................................28C..........................279D............................................................31DB131081.1-2009JDB13/T10813112V-341,3-..567891011111213A143,3(342151,31617181,21,31,44,4'4,4'192N,N2021222324254126I272,4,61,3,5281,1,129163063123DB3811DDCEN/TS131302005A,}%13,C,1)DB13/T1081.1-20091HiI...-il-DB13/T1081.1-200912002/72/EC2FEN10088Part1ENISO8442-2:1997Part2ISO8442-2:1997)ISO648ISO4788ISO572533.1plastics3.2finalmaterialrticle3.3sample3.4testspecimen3.5testpiece3.6conventionalovenDB13/T1081.1-20093.7foodstimulant4-7)3.8specificmigration3.9compositionalcontent3.10specificmigrationlimit(SML)3.11SML(T)3.12residuallimit(Qm)3.13Qm(T)moiety3.14QMAmg/6dm3.15reductionfactor253.16migrationtest3.17substitutefattesttestmedia)3.18testmedia953.19alternativefattestDB13/T1081.1-20093.20volatiletestmedia3.21extractiontest3.22dissolutiontest3.23pouchtestmedium)3.24reversepouch1htestmedium3.25celltestmedium3.26repeatabilityvaluerISO5724953.27reproducibilityvalueRISO572595%3.283.2944.111.DB13IT1081.1-2009testmedium4.2AAJABS),4.34.44.5testmediumsubstitutefattests),954.6alternativefattestAT-4.7mg/kgmg/6dm24.8M4.9(Qm,mg/kg)J.J..44.1.l_J.M.o5.1DB13/T1081.1-20096.16.2105.2(substitutetest),testmedium.Testmedium954,2-566.2)5.3Alternativefattests5.3.1.l4r5.3.2Alternativetest95Alternativetesta)Alternativetestb)Alternativetest5.3.3D)5.45.4.1(Qmtest)Vmgkgmg/kg.5.4.2QMAtest)QMAQmQMA6dmZmgmg/6dm`Qm5.4.2.1QMA0.25mm0.25mmQMA0.25mmD0.25mm01..iD/0.25)1mmu-W.405.4.2.2QMA0.25mmQMA5.4.2.3QMA0.25mm0.25mmDB13/T1081.1-200966.1A3%(W/vB30g10%(v/vC100mL1L106.2DDDBDB1B27.3206.3testmedium6.3.1testmediaforsubstitutetest95B.6.3.2Alternativetestalternativetest95Y-JX6.477.185/572/EEC15(v/v)C97/48/EC10(v/v)7.23w/v).10v/v)D7.3a)bDB13/T1081.1-2009c)1)2b)1a)c)21ABCDBCCBDADBDCD.CB2ABCD0101.015%X(a)X(a)01.025%xaXb01.03xaXb0202.01t02.0202.0302.04ff02.053X/5DB13/T1081.1-200902.06X/5DB13/T1081.1-20092ABCD0303.0103.022)3XX15X/303.03m3xX0404.01T04.0231)2)3(5%X(a)X(a)X(a)X(a)X(a)X(a)X(a)XX04.033XX15CX/3c04.04VDB13/T1081.1-20092ABCD04.05ABC1)2)3_5X(a)X(a)X(a)X(a)X(a)X(a)XaxX0505.01XX/20606.013XXX/3cX/3c06.02ax06.03A3XXX/4X/406.04XX/406.05A:3X(a)X(a)X(a)X(a)X06.063X06.073X06.0807DB13/T1081.1-20092(ABCD07.013X07.02X07.03X(a)X(a)07.04A3X(a)X(a)X(a)XaX/3`07.05A3X(a)X(a)0808.01X08.02ABX/5X/408.03A1)2B1)2X(a)X(a)X(a)X(a)X/5X/308.043X(a)X(a)08.059DB13/T1081.1-20092ABCD08.06ABCX(a)X(a)X(a)X(a)X(a)X(a)X/3X08.07X(a)X(a)X/3`08.08ABX/508.09X08.10ABX/508.1108.125xax08.13AAJAJBX/5`X/3`08.1408.15X08.1608.171:XX2:X/55ReductionFactor);3:X(a)pH4.5ApH-4.5B4:apH-4.55:b10%6:D7.4A,B.CDMPPODB13/T1081.1-20097.50fanycontact)DTC194EN144818alternative8.18.1.182/811/EECC.1C.28.1.233t5min8.1.75mint0.5h0.5h0.5ht1hlh1ht2h2h2ht4h4h4ht24h24ht24h10dT5¡ãC55¡ãCT20¡ãC20¡ãC20¡ãCT40¡ãC40¡ãC40¡ãCT70¡ãC70¡ãC70¡ãCT100¡ãC100¡ãC100¡ãCT121¡ãC121¡ãCa121¡ãCT130¡ãC130¡ãCa130¡ãCT150¡ãC150¡ãCaT150¡ãC175¡ãCaDA,BC100¡ãC8.