SNT 1405-2004 进出口蜂产品中10-羟基-α癸烯酸的检验方法 毛细管电泳法

110---Inspectionof10-hydroxy--decenoicacidinbeeproductsforimportandexportCapillaryelectrophoresismethodSNT14052004A110---(10-HDA)10---(10-HDA)22.11000kg250kg2.2112l505110010057102.32.2()20g2.4-1833.110-HDA3.23.2.13.2.20.03molL3.2.399.03.2.40.65g(0.0002g)1000mL0.65mg3.2.5(SDS)3.2.6()3.2.7(pH9.2)2.86g(3.2.6)0.718gSDS(3.2.5)100mL0.075molLSDS0.025molL33.2.810-HDA99.024h3.2.910-HDA10-HDA0.025g(0.0002g)25mL10-HDA1mg3.33.3.13.3.23.3.33.3.44000rmin16000rmin3.3.515mL1.5mL3.43.4.10.5g(.001g)50mL2mL(3.2.2)30mL(3.2.)10.0mL(3.2.4)15min15mL3000rmin10min.0.5mL1.5mL0.5mL(3.2.7)16000rmin10min3.4.20.15g(0.001g)50mL20mL(3.2.1)2mL(3.2.2)10.0mL(3.2.4)15min15mL3000rmin10min0.5mL1.5mL0.5mL(3.2.7)16000rmin10min3.50.5mL1.0mL2.0mL3.0mL4.0mL5.0mL10-HDA(3.2.9)10mL2.0mL(3.2.4).0.5mL0.5mL(3.2.7)43.610-HDA17.9min2l.7minA.14a)75m()57cm50cmb)3.2.7c)210nmd)0.5Pae)5sf)25g)15kV5(1)(1)FAiAs10-HDAmi(mg)ms10-HDA(mg)(2)10-HDA(2)5X10-HDAA1A210-HDAm1(mg)m2(mg)()2lA()6